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The morphology of sheep wool applied as organic fertilizer biodegraded in the soil was examined. The investigations were conducted in natural conditions for unwashed waste wool, which was rejected during sorting and then chopped into short segments and wool pellets. Different types of wool were mixed with soil and buried in experimental plots. The wool samples were periodically taken and analyzed for one year using Scanning Electron Microscopy (SEM) and Energy-dispersive X-ray Spectroscopy (EDS). During examinations, the changes in the fibers' morphology were observed. It was stated that cut wool and pellet are mechanically damaged, which significantly accelerates wool biodegradation and quickly destroys the whole fiber structure. On the contrary, for undamaged fibers biodegradation occurs slowly, layer by layer, in a predictable sequence. This finding has practical implications for the use of wool as an organic fertilizer, suggesting that the method of preparation can influence its biodegradation rate. (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(SEM)(sic)(sic)(sic)(sic)(sic)X(sic)(sic)(sic)(sic)(EDS)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic).

期刊论文 2025-12-31 DOI: 10.1080/15440478.2024.2446947 ISSN: 1544-0478

The erosion of cohesive soils is regarded as one of the major threats to the failure of earth structures. The current evaluation of clay erodibility is primarily based on empirical correlations with other physical and mechanical soil properties, which lack a fundamental understanding of multiscale resistance formation under complicated environmental conditions. In this study, the hole erosion test (HET) was conducted using our augmented testing system, which includes sample preparation equipment and a temperature control unit. The kaolinite specimen is prepared following the saturated preconsolidation approach under defined stresses, which significantly improves the test repeatability. In total, 33 specimens are prepared and tested using the enhanced HET system under varying preconsolidation pressures, temperatures, and fines contents with triplicates for each case. The erosion resistance of clay increases with the preconsolidation pressure, and macropores are destructed into micropores, as revealed by the mercury intrusion porosimetry (MIP) test and the specific surface area analyzer. The scanning electron microscopy (SEM) images indicate an anisotropic aggregate structure prepared using the preconsolidation approach, which possesses different erodibility indices in different flow directions. With the increase in temperature from 10 degrees C to 40 degrees C, the critical shear stress decreases from 292 to 131 Pa (or by 55.1%). The addition of quartz sands in the kaolinite clay undermines the soil erosion resistance.

期刊论文 2025-06-01 DOI: 10.1061/IJGNAI.GMENG-10504 ISSN: 1532-3641

This study explores a novel stabilization technique combining Persian gum (PG), an eco-friendly biopolymer, and glass fiber (GF) to enhance the strength and durability of fine-grained soils under freeze-thaw (F-T) cycles. Specimens were prepared at maximum dry density (MDD) with varying PG and GF contents, cured for 0, 7, or 14 days, and subjected to 0, 5, 7, or 10 F-T cycles. Tests included Standard Proctor compaction, Scanning Electron Microscopy (SEM), Unconfined Compressive Strength (UCS), and Direct Shear (DS). Results demonstrated that GF significantly improved durability, ductility, and strength by enhancing interparticle interaction and friction angle. The results indicated that at an optimum GF content of 1%, UCS and E-5(0) increased by up to 35%. Also, after 10 F-T cycles, UCS decreased by 46% for untreated soil and 36% for treated soil. PG enhanced cohesion through interparticle bonding, which was curing-time-dependent. Specimens with 2.5% PG (optimum content) showed a 133% UCS increase after 14 days of curing but a 9% reduction after 5 F-T cycles, with 70% of total UCS loss occurring in the first 5 cycles. The tests indicated that formation of large and stable soil-PG-GF matrix with improved rigidity, strength, and F-T resistance. The results demonstrated that the suggested soil stabilization method, which utilizes low-cost, eco-friendly materials, was effective.

期刊论文 2025-06-01 DOI: 10.1007/s10706-025-03179-y ISSN: 0960-3182

Fissured loess slopes along the railway in the Loess Plateau frequently suffer from disintegration disasters under the coupled effects of rainfall and train vibrations, causing soil collapse that covers tracks and severely threatens railway safety. To reveal the disaster mechanisms, this study conducted water-vibration coupled disintegration tests on fissured loess using the self-developed EDS-600 vibration disintegration apparatus, based on the measured dominant vibration frequencies (12-46 Hz) of the Lanzhou-Qinghai Railway. The influence patterns of vibration frequency (f) and fissure type (t) on disintegration rate (S), disintegration velocity (V), and disintegration velocity growth rate (\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$\alpha_{f - t}$$\end{document}) were systematically investigated, with scanning electron microscopy (SEM) employed to uncover microstructural evolution mechanisms. Results indicate that vibration frequency and fissure type significantly accelerate disintegration: V reaches its maximum at f = 20 Hz, and under the same frequency, V increases with the growth of fissure-water contact area. Under two fissures and f = 20 Hz, V increases by 225% compared to the without vibration and fissures scenario, with the \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$\alpha_{f - t}$$\end{document} value peaking at 137.23% and the synergistic effect index exceeding the single-factor superposition value by 45.99%. Microscopically, water-vibration coupling disrupts clay mineral cementation, reconstructs pore networks, and forms dominant seepage channels, leading to reduced interparticle bonding strength, heterogeneous water film distribution, and stress concentration, thereby inducing fractal propagation of secondary fissures and shortening moisture absorption and softening stages. Combined with unsaturated soil mechanics theory, the study reveals a cross-scale progressive failure mechanism involving simultaneous degradation of matric suction, cementation force, and macroscopic strength. A theoretical framework integrating vibration energy transfer, seepage migration, and structural damage is established, along with a quantitative relation linking vibration frequency, fissure parameters, and disintegration velocity. This provides multi-scale theoretical support for disaster prevention and control of railway slopes and foundations in loess regions.

期刊论文 2025-05-20 DOI: 10.1038/s41598-025-01391-7 ISSN: 2045-2322

The use of various sustainable materials and cement is a frequent and successful strategy for stabilizing problematic soil. The current research discusses the potential use of discarded millet husk ash (MHA) and cement (C) as subgrade ingredients to improve the geotechnical qualities of soil (S). MHA and cement are mixed in different proportions and the engineering characteristics of the stabilized soil are studied. The study involves examining fundamental properties, such as specific gravity and Atterberg's limits, as well as engineering properties, including Unconfined Compressive Strength (UCS) and California Bearing Ratio (CBR) tests. These evaluations are conducted to assess the feasibility of using the MHA-cement blend as a construction material. Additionally, FTIR & SEM analysis shows the addition of MHA-cement blend effectively couples with the soil. The test findings demonstrate that adding MHA to soil lead to decreased liquid limits and plasticity indices. The maximum dry density (MDD) was observed to decrease when MHA was mixed with soil. When 8% cement was incorporated to the S:MHA (84.5:7.5) combination, the UCS value rose even higher reaching 1600.1 kPa. The S:MHA:C arrangement in the ratio of 84.5:7.5:8 had the greatest California bearing ratio (CBR). Fourier transform infrared spectroscopy (FTIR) elucidated the various types of bond formations present within the soil composite and deeper peaks depicted greater presence of cementitious compounds after curing period. SEM analysis exhibited a greater density of N-A-S-H and C-A-S-H gels in comparison to natural soil samples. The findings suggest that the MHA-cement blend can effectively enhance the geotechnical properties of problematic soils, while addressing issues of agricultural waste management. This research contributes to several Sustainable Development Goals (SDGs), including SDG 9 (Industry, Innovation, and Infrastructure) by promoting innovative construction materials.

期刊论文 2025-05-20 DOI: 10.1007/s40098-025-01243-1 ISSN: 0971-9555

In aggressive environments, including acidic environments, low and high-plasticity clays play an important role in transmitting and spreading dangerous pollution. Stabilisation of these types of soils can improve their characteristics. In this research, different ratios of two precursors with a low calcium percentage, for example, waste statiti-ceramic sphere powder (WS-CSP) and a high calcium percentage (e.g. ground granulated blast furnace slag [GGBFS], were employed to investigate the properties of soils with different plasticity indices [PIs]). Low and high-plasticity-stabilised and stabilised with 5 wt% Portland cement specimens were prepared and exposed to an acidic solution with a pH of 2.5 in intervals of 1, 3, 6 and 9 months. The long-term durability of specimens was evaluated using the uniaxial compressive strength test (UCS) and bending strength test (BS). Additionally, the microstructures of these specimens under various time intervals were analyzed using scanning electron microscopy and Fourier-transform infrared. According to the results, in an acidic environment, the reduction in UCS, BS, toughness and secant modulus of elasticity (E50) for low-plasticity-stabilised specimens and containing 100% WS-CSP was lower than that of other specimens. The Taguchi method and ANOVA were used to investigate the effect of each control factor on the UCS and BS.

期刊论文 2025-04-30 DOI: 10.1080/19648189.2025.2496349 ISSN: 1964-8189

Coastal regions often face challenges with the degradation of cementitious foundations that have endured prolonged exposure to corrosive ions and cyclic loading induced by environmental factors, such as typhoons, vehicular traffic vibrations, and the impact of waves. To address these issues, this study focused on incorporating Nano-magnesium oxide (Nano-MgO) into cemented soils to investigate its potential impact on the strength, durability, corrosion resistance, and corresponding microstructural evolution of cemented soils. Initially, unconfined compressive strength tests (UCS) were conducted on Nano-MgO-modified cemented soils subjected to different curing periods in freshwater and seawater environments. The findings revealed that the addition of 3% Nano-MgO effectively increased the compressive strength and corrosion resistance of the cemented soils. Subsequent dynamic cyclic loading tests demonstrated that Nano-modified cemented soils exhibited reduced energy loss (smaller hysteresis loop curve area) under cyclic loading, along with a significant improvement in the damping ratio and dynamic elastic modulus. Furthermore, employing an array of microscopic analyses, including nuclear magnetic resonance (NMR), X-ray diffraction (XRD), and scanning electron microscopy (SEM), revealed that the hydration byproducts of Nano-MgO, specifically Mg(OH)2 and magnesium silicate hydrates, demonstrated effective pore space occupation and enhanced interparticle bonding. This augmentation markedly heightened the corrosion resistance and durability of the cemented soil.

期刊论文 2025-04-01 DOI: 10.1061/JMCEE7.MTENG-18603 ISSN: 0899-1561

The impact of four distinct calcium sources on the microbial solidification of sand in the Kashi Desert, Xinjiang, was investigated. A wind tunnel test over a 60-day period revealed the cracking behavior of four different complex calcium nutrient solutions. By comparing the bearing capacity and the results from dry-wet cycling and freeze-thaw cycle tests, it was concluded that the sample treated with calcium gluconate exhibited superior sand fixation performance, whereas the sample treated with calcium acetate showed weaker sand fixation effects. The microstructure of the treated sand samples was analyzed using scanning electron microscopy (SEM) and X-ray diffraction (XRD). Elemental analysis was conducted via energy dispersive spectroscopy (EDS), and functional groups were identified through Fourier transform infrared spectroscopy (FTIR). These experimental findings hold significant implications for soil remediation, pollutant removal in soil, enhancement of soil fertility, and desert soil stabilization.

期刊论文 2025-03-17 DOI: 10.1038/s41598-025-94124-9 ISSN: 2045-2322

This paper investigates the anisotropic characteristics of Champlain marine clay soil using a combination of laboratory techniques. A modified oedometer cell with a piezoelectric ring actuator technique was used to measure shear wave velocity during consolidation stages. The axisymmetric design of the oedometer allowed for the determination of shear wave velocity in both the vertical and horizontal planes. The preliminary findings reveal that the sensitive marine clay is inherently anisotropic, with lower preconsolidation pressure for horizontally consolidated specimens and faster propagation of shear waves in the plane parallel to the bedding layer. High-precision strain gauges integrated into the consolidation ring were used to evaluate horizontal stress during the one-dimensional consolidation test. The ability to determine mean effective stress enables the normalization of shear wave velocities using this stress, providing more coherent empirical correlations in terms of shear wave velocity. Scanning electron microscopy was used to examine the microstructure of clay specimens, providing qualitative and quantitative insight into the restructuring and reorientation of clay platelets under consolidation stress. The consistency of the results through both micro and macro-scale analyses confirms the reliability of the experimental approach, highlighting its potential for future studies on the anisotropy of Champlain marine clay fabrics.

期刊论文 2025-01-01 DOI: 10.1139/cgj-2024-0163 ISSN: 0008-3674

Cement reinforcement can effectively mitigate the frost heave and thaw settlement in soft clay during artificial ground freezing. Generally, soft clay has strong creep characteristics, which is also the main factor influencing the construction safety in coastal area. However, the mechanism of freeze-thaw action with cement reinforcement on the creep is really unclear. In this paper, the creep characteristics of cemented-soil after freeze-thaw have been investigated through triaxial creep test, and the micro-mechanism has been explored by Scanning Electron Microscopy (SEM) test and PFC numerical simulation. Three quantitative parameters of porosity, average particle size, and particle roundness have been extracted from SEM pictures. The results showed that creep deformation of cemented-soil is higher after freeze-thaw than before, with an increase as the freezing temperature drops. When combining freezing with cement reinforcement, there is an overall decrease in the creep behavior. It was observed from numerical simulation that the slip deformation of cemented-soil particles is generated from top to bottom and from outside in. Moreover, the porosity of cemented-soil increased from 24.5 to 28.5%, the particle roundness decreased from 2.11 to 1.75, while average particle size decreases from 16.67 to 13.88 mu m during creep process. These shifts are explained by particles sliding and disordering, with debris migrating to the interior of pores. The results provide a scientific reference for the development of underground space in the coastal area.

期刊论文 2025-01-01 DOI: 10.1007/s12665-024-11964-w ISSN: 1866-6280
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