Lunar soil, as an in-situ resource, holds significant potential for constructing bases and habitats on the Moon. However, such constructions face challenges including limited mechanical strength and extreme temperature fluctuations ranging from -170 degrees C to +133 degrees C between lunar day and night. In this study, we developed a 3D-printed geopolymer derived from lunar regolith simulant with an optimized zig-zag structure, exhibiting exceptional mechanical performance and thermal stability. The designed structure achieved remarkable damage tolerance, with a compressive strength exceeding 12.6 MPa at similar to 80 vol% porosity and a fracture strain of 3.8 %. Finite element method (FEM) simulations revealed that the triangular frame and wavy interlayers enhanced both stiffness and toughness. Additionally, by incorporating strategically placed holes and extending the thermal diffusion path, we significantly improved the thermal insulation of the structure, achieving an ultralow thermal conductivity of 0.24 W/(m K). Furthermore, an iron-free geopolymer coating reduced overheating under sunlight by 51.5 degrees C, underscoring the material's potential for space applications.
In situ resource utilization of lunar regolith provides a cost-effective way to construct the lunar base. The melting and solidifying of lunar soil, especially under the vacuum environment on the Moon, are the fundamentals to achieve this. In this paper, lunar regolith simulant was melted and solidified at different temperatures under a vacuum, and the solidified samples' morphology, structure, and mechanical properties were studied. The results indicated that the density, compressive strength, and Vickers hardness of the solidified samples increased with increasing melting temperature. Notably, the sample solidified at 1400 degrees C showed excellent nanohardness and thermal conductivity originating from the denser atomic structure. It was also observed that the melt migrated upward along the container wall under the vacuum and formed a coating layer on the substrate caused by the Marangoni effect. The above results proved the feasibility of employing the solidified lunar regolith as a primary building material for lunar base construction.
H2O extraction from remote icy lunar regolith using concentrated irradiation was investigated under high-vacuum and low-temperature conditions. The thermal sublimation of H2O(s) from packed beds of lunar regolith simulants was quantified with and without an indirect solar receiver for average concentrated irradiations of 37.06 f 2.66 and 74.62 f 3.57 kW/m2. The indirect solar receiver increased sublimation by an average of 18.7 % f 10.4 %, despite slower heating rates due to its increased thermal mass. Different average concentrated irradiations affected the heating rates and thermal gradients within the packed bed, but the impact on overall sublimation was not statistically significant. An inverse relationship between heating rates and normalized sublimation was also observed, where rapid sublimation near the heating elements led to the formation of a desiccated layer of regolith, which behaved as a thermal insulator and further limited heat transfer, reducing the sublimation efficiency. These findings provide key insights for optimizing in-situ resource utilization technologies, contributing to the development of efficient methods for extracting H2O from lunar regolith, which is essential for sustainable space exploration.
The lunar base establishing is crucial for the long-term deep space exploration. Given the high costs associated with Earth-Moon transportation, in-situ resource utilization (ISRU) has become the most viable approach for lunar construction. This study investigates the sintering behavior of BH-1 lunar regolith simulant (LRS) in a vacuum environment across various temperatures. The sintered samples were characterized using X-ray diffraction (XRD) and scanning electron microscopy (SEM), along with nanoindentation, uniaxial compression, and thermal property tests to evaluate the microstructural, mechanical, and thermal properties. The results show that the sintering temperature significantly affects both the microstructure and mechanical strength of the samples. At a sintering temperature of 1100 degrees C, the compressive strength reached a maximum of 90 MPa. The mineral composition of the sintered samples remains largely unchanged at different sintering temperatures, with the primary differences observed in the XRD peak intensities of the phases. The plagioclase melting first and filling the intergranular pores as a molten liquid phase. The BH-1 LRS exhibited a low coefficient of thermal expansion (CTE) within the temperature range of - 150 degrees C to 150 degrees C, indicating its potential for resisting fatigue damage caused by temperature fluctuations. These findings provide technical support for the in-situ consolidation of lunar regolith and the construction of lunar bases using local resources.
In-Situ Resource Utilization (ISRU) approaches hold significant importance in plans for space colonization. This work explores a different ISRU concept applying fast-firing, a robust and well-known industrial process, to Mars regolith simulant (MGS-1). The fast-fired specimens were compared to the ones obtained by conventional sintered under low heating rates. When the holding time at the firing temperature is longer than 15 min, fast-fired specimens exhibited higher density and flexural strength (> 35 MPa) than conventional sintering. For both processes, the bulk density values and the mechanical properties of the regolith compacts were enhanced with increasing dwell time. This was attributed to higher heating rates changing the densification/crystallization kinetics involving the basalt glass in the regolith composition. Specifically, high heating rate promotes sintering over crystallization. On these bases, fast firing can be considered a potential candidate for ISRU on Mars.
The Moon, as the celestial body closest to Earth, is a prime target for human deep space exploration. China's Lunar Exploration Project IV aims to explore and sample the lunar polar region's water-containing regolith. To effectively simulate the characteristics of this watery lunar regolith, this paper proposes a deep low-temperature preparation system. The feasibility of the system design is validated through theoretical and methodological analysis, including cold source selection, heat dissipation analysis, and energy consumption calculations. Subsequently, a deep low-temperature aqueous lunar regolith preparation system was developed, and tests were conducted to verify its performance. The results confirm that the system can generate water-containing lunar regolith at -238 degrees C and maintain its temperature during drilling. This capability is significant for subsequent research on the drilling performance of deep low-temperature watery lunar regolith.
Preparing regolith-based composites for 3D printing is crucial in lunar base construction, leveraging costeffective and mechanically favorable materials for lunar construction by utilizing lunar regolith as the reinforcing phase. This research focuses on developing lunar regolith simulant as a matrix for 3D printing, which is crucial for in-situ resource utilization on the Moon. Resin-based composites, well-established in aerospace, are explored for their simple manufacturing and robust properties. The formulation involves simulated regolithbased polymer for direct ink writing printing. Rheological properties, including yield stress and plastic viscosity, are characterized across various cementite-sand ratios and printing temperatures. The relationship between extrudability, the time interval of the printing material and its rheological attributes is investigated. Quantitative assessment of material buildability employs three-dimensional scanning of the printed parts. Freeze-thaw cycle tests explore its temperature resilience. The influence of varying the printing infill rate on printing efficiency and the performance of the printed parts was assessed. It was found that modulating the printing infill rate affects the efficiency and performance of parts, with a 1:4 cementite-sand ratio and a 40 degrees C print temperature demonstrating optimal printing workability. These findings offer an efficient scheme for the automated production of regolithbased epoxy composites with precise structural, temperature-resistant, and favorable mechanical properties.
The technology of 3D printing, referred to as additive manufacturing, is widely acknowledged as a transformative innovation that has the potential to supplant traditional processing methods in numerous domains. The present study showcases a quantitative assessment of the mechanical properties of moon dust, also known as Lunar Regolith Simulants (LRS), printed through vat polymerization. In this study, we conduct a thorough investigation and explore the effects of layer height [LH] (LH = 10 mu m, 20 mu m, 30 mu m, 40 mu m, 50 mu m, 60 mu m]), exposure time [ET] (ET = 3000 ms, 5000 ms, 7000 ms, 11,000 ms), and sintering impact [1075 degrees C, 1082 degrees C, 1083 degrees C, 1085 degrees C, 1086 degrees C, 1087 degrees C, 1090 degrees C] on the mechanical properties of printed structures. Herein, we utilize a 55 % volume suspension of LRS to print rod and block configurations via digital light printing [DLP] that are subsequently consolidated through sintering in ambient air. This 55 % LRS via vat polymerization approach has not been previously reported. The morphology of the simulant powders exhibited irregular and angular features. Our experimental results show that a 30 um (LH) with (ET) 11,000 ms exhibits maximum compressive and flexural strength of 330 MPa and 100 MPa at 1085 degrees C. The sintering atmosphere greatly affects the microstructure, macroscopic features, and mechanical strength of 3D-printed LRS, which reveals diverse chemical compositions and underlying reaction mechanisms. This sintering process improves particle bonding, resulting in densification and reduced voids within the 3D-printed structure. It is essential to optimize the annealing parameters to achieve the desired strength while avoiding excessive sintering that may cause dimensional distortions or structural defects. This innovative approach opens new possibilities for future space exploration and extraterrestrial construction.
The mechanical and thermal properties of the fabricated structures composed of lunar regolith are of great interest due to the urgent demand for in situ construction and manufacturing on the Moon for sustainable human habitation. This work demonstrates the great enhancement of the mechanical and thermal properties of CUG-1A lunar regolith simulant samples using spark plasma sintering (SPS). The morphology, chemical composition, structure, mechanical and thermal properties of the molten and SPSed samples were investigated. The sintering temperature significantly influenced the microstructure and macroscopic properties of these samples. The highest density (similar to 99.7%), highest thermal conductivity (2.65 W.m(-1).K-1 at 1073 K), and the best mechanical properties (compressive strength: 370.2 MPa, flexural strength: 81.4 MPa) were observed for the SPSed sample sintered at 1273 K. The enhanced thermal and mechanical properties of these lunar regolith simulant samples are attributed to the compact structure and the tight bonding between particles via homogenous glass.
The development and utilization of lunar resources are entering a critical stage. Immediate focus is needed on key technologies for in-situ resource utilization (ISRU) and lunar base construction. This paper comparatively analyzes the basic characteristics of lunar regolith samples returned from Chang'e-5 (CE- 5), Apollo, and Luna missions, focusing on their physical, mechanical, mineral, chemical, and morphological parameters. Given the limited availability of lunar regolith, more than 50 lunar regolith simulants are summarized. The differences between lunar regolith and simulants concerning these parameters are discussed. To facilitate the construction of lunar bases, this article summarizes the advancements in research on construction materials derived from lunar regolith simulants. Based on statistical results, lunar regolith simulant-based composites are classified into 5 types by their strengthening and toughening mechanisms, and a comprehensive analysis of molding methods, preparation conditions, and mechanical properties is conducted. Furthermore, the potential lunar base construction forms are reviewed, and the adaptability of lunar regolith simulant-based composites and lunar base construction methods are proposed. The key demands of lunar bases constructed with lunar regolith-based composites are discussed, including energy demand, in-situ buildability, service performance, and structural availability. This progress contributes to providing essential material and methodological support for future lunar construction. (c) 2024 Published by Elsevier B.V. on behalf of China University of Mining & Technology. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).